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1-25 of 62 Business Insights

  • Application Note

    Transport of Nanoparticles from Coated Surfaces through Physical Contact

    This work investigated the transfer of Ag and CuO nanoparticles from consumer products via simulated dermal contact by using textile wipes as a surrogate using PerkinElmer’s NexION® ICP-MS single particle analyzer with the unique Syngistix Nano Application software module for data collection and analysis.

  • Application Note

    Analysis of Single-Walled Carbon Nanotubes with SP-ICP-MS

    Measuring the amount of metals in CNTs presents a challenge. High levels can be measured directly in the solid by several techniques, including XRF and TEM, while low-level analysis requires complete digestion of the sample prior to analysis by ICP-OES or ICP-MS.

  • FAQ

    Syngistix for ICP Enhanced Security Software for Laboratories Subject to 21 CFR Part 11 Regulations

    The regulations of 21 CFR Part 11 cover overall system compliance and include administrative, procedural and technical elements. Software alone cannot be compliant without the development and implementation of the other elements. PerkinElmer’s Syngistix? for ICP Enhanced Security? software for Avio? and Optima? ICP-OES systems provides features that, when coupled with appropriate policies and procedure, fulfill the requirements for closed-system electronic records in 21 CFR Part 11. Syngistix Enhanced Security software also fulfills the elements relating to electronic signatures.

  • Application Note

    Analysis of Impurities in Aluminum with the Avio 200 ICP-OES Following London Metal Exchange Guidelines

    Due to aluminum’s varied uses and popularity, there are many grades available. The London Metal Exchange (LME) lists specifications for two commonly-used aluminum (Al) purities: 99.5% and 99.7%1, with each having up to six inorganic impurities specified. ICP-OES is the best technique for measuring these impurities at these levels due to its ability to easily handle high-matrix samples and simplicity of operation.

    This work describes the analysis of impurities in Al at the LME specifications using the Avio® 200 hybrid scanning ICP-OES, an ideal choice for this application – its optical design provides excellent light throughput, essential for measuring lower concentrations with shorter analytical times, plus, its charge-coupled device (CCD detector) provides simultaneous background and analyte measurement, important for samples such as metal matrices.

  • Application Note

    Analysis of Soils and Waters Following U.S. EPA Method 6020B using the NexION 2000 ICP-MS

    Through the years, both industry and analytical instrumentation have advanced. With the development of new chemicals and processes, new pollutants may enter the environment. However, the capabilities of analytical instruments have also increased, allowing the measurement of ever lower levels of environmental contaminants, as well as new pollutants.

  • Application Note

    Determination of Trace Elements in Eye Drops with the NexION ICP-MS

    Eye drops are commonly used medications which are available both over-the-counter and as prescriptions in various forms. Because eye drops are classified as a parenteral medication and have relatively large daily doses, the inorganic components in eye drops must be present at low concentrations. As a result, ICP-MS is the most appropriate technique for the determination of trace elements in eye drops.

    The International Conference on Harmonization Guideline for Elemental Impurities Q3D (ICH Q3D) has established maximum permitted daily exposure limits for elemental impurities in pharmaceutical products. This work discusses the sample preparation and analysis of Class 1, 2, and 3 elements in a variety of eye drops with the NexION ICP-MS, following the criteria defined in ICH Q3D. The developed methodology (both sample preparation and analytical) demonstrates both accuracy and stability.

  • Application Note

    The Application of ASTM Standard D7720 to Used Oil Data Using TIBCO Spotfire?

    The importance of managing and utilizing such data is emphasized by the creation of ASTM standard D7720, Statistically Evaluating Measurand Alarm Limits when Using Oil Analysis to Monitor Equipment and Oil for Fitness and Contamination. This application note demonstrates the transformation of used oil data in accordance with the aforementioned ASTM standard using data visualization software program TIBCO Spotfire?.

  • Application Note

    Analysis of Aluminum Alloys with the Avio 200 ICP-OES Following London Metal Exchange Guidelines

    Due to its unique characteristics, aluminum (Al) is used in a wide variety of commercial and industrial applications. Its utility can be further enhanced by combining it with other metals to create aluminum-based alloys, where the non-aluminum additives can make up to 15% of the total alloy, by weight.

    Because of its popularity and multiple compositions, the London Metal Exchange (LME) lists four different specifications for Al alloy compositions. In these specifications, silicon, copper, zinc, and iron are considered major additions, as they are mostly greater than 1% composition by weight. Therefore, these four elements must be determined with greater accuracy (± 2%) than the others.

    This work describes the determination of additives to Al in aluminum alloys at the LME specifications using the Avio® 200 hybrid scanning ICP-OES, an ideal choice for labs performing this application thanks to its charge-coupled device (CCD) detector, providing simultaneous background and analyte measurement, important when dealing with complex matrices, such as alloys.

  • Application Note

    Analysis of Micronutrients in Milk Using the Avio 200 ICP-OES

    With its great importance, milk is available in several different forms: fresh, boxed (ultraheat treated), powdered, and evaporated. The most commonly consumed form varies globally, being dependent on factors such as geography, culture, and climate. For milk producers, internal quality control and the possibility of external monitoring provide strong incentives for the ability to quickly, accurately, and easily monitor nutrients in their products.

  • Application Note

    Speciation of Hexavalent Chromium in Children's Toys According to EN 71-3 Category II with the NexSAR HPLC-ICP-MS

    Testing for harmful metal(loid)s that may be included in raw materials, processes, paints and additives used in the manufacturing processes of children's toys has been mandated by the regulation EN 71-3. This regulation recommends specific testing methods and maximum allowable concentrations of leachable metals and metalloids such as Al, As, B, Ba, Cd, Co, Cr (III), Cr (VI), Cu, Hg, Mn, Ni, Pb, Sb, Se, Sn, organotin, Sr and Zn in parts of toys, with the exclusion of general packaging materials.

    This work shows a method for the measurement of hexavalent chromium in different toy material categories in accordance with method EN 71-3 Category II, leveraging the unique combination and capabilities of the NexSAR Inert HPLC coupled to the robust NexION® ICP-MS.

  • Flyer

    5 Tips to Improving Your Sample Digestion

    Sample preparation is one of the most critical steps in your analytical process. Often accounting for 60% of your analytical timetable, it has a fundamental impact on laboratory throughput and analytical performance. Any errors within the sample preparation process will undermine the quality of your food data at all subsequent stages of your analysis. Here are five tips to improving your sample digestion for food samples.

  • Application Note

    Analysis of Milk for Major and Trace Elements by ICP-MS

    Milk and milk powder are used widely in the food industry for the production of other foods. Because of its nutritional importance and widespread consumption, regulations in many countries necessitate that the quality of the milk is routinely monitored.

  • Application Note

    Analysis of Oil Additives Following ASTM D4951 with the Avio 200 ICP-OES

    When blending base oils and additives for use as lubricants, it is important to know and control the concentrations of certain elements for optimal performance and longer engine life. This work will focus on the analysis of additives in new oils using PerkinElmer’s Avio? 200 ICP Optical Emission Spectrometer (ICP-OES), which overcomes limitations of other ICP-OES systems and X-ray analyses.

  • Application Note

    Advantages of a High Throughput Sample Introduction System in the Analysis of Drinking Waters Using ICP-MS (Method 200.8)

    The most significant challenges of trace element analysis of drinking water is ensuring detection capability that comply with the regulatory framework at the same time as maximising sample throughput. The NexION 1000 ICP-MS solves the challenges that high throughout laboratories face using a robust, simple method and a single gas mixture. This note explains how the NexION exceeds expectations on detection capability and details the benefits of using the single gas mixture for a wide range of elements, even those where the first ionisation energy is relatively high (e.g. selenium).

  • Application Brief

    Arsenic Speciation Analysis in Rice Following Method GB 5009.11-2014 to Ensure Safety

    Rice represents a dietary staple for over half of the world's population. However, in recent years, concerns have been raised over the presence of high levels of arsenic (As), where this carcinogenic metalloid can be accumulated at levels far exceeding ambient concentrations. Since China is the world's largest producer of rice, the Chinese government released a national standard method in 2014 for food safety – GB 5009.11– to aid the evaluation of As species in rice and rice products. In this document, HPLC-ICP-MS is identified as the preferred analytical technique.

    In this study, five arsenic species were characterized in a commercial rice sample and certified reference material using a gradient anion-exchange method in accordance with GB 5009.11. The analysis was performed using a PerkinElmer NexSAR HPLC-ICP-MS speciation solution, consisting of a NexSAR inert HPLC coupled to a NexION® ICP-MS.

  • Brochure

    OilExpress 4 Oil Condition Monitoring System

    The OilExpress 4 system adapts to your laboratory’s needs, from dozens to thousands of samples per day. Its modular design makes it possible to scale up your sample throughput or separately utilize the oil dilution capabilities in busy laboratories that are using ICP analysis. The system minimizes your operational costs by reducing instrument downtime, increasing throughput to reduce cost per sample, and offering significant savings from decreased solvent waste.

  • Application Note

    Analysis of Allergy Medications Using ICP-OES Following USP 232/233 Guidelines with Software Designed to Aid in 21 CFR Part 11 Compliance

    This work demonstrates the ability of the Avio 500 ICP-OES to meet the USP <232>/<233> criteria for the analysis of orally-administered allergy tablets using Syngistix for ICP Enhanced Security software version 4.0, which provides the tools to help laboratories meet 21 CFR Part 11 compliance.

  • Brochure

    Avio 200 Inductively Coupled Plasma Optical Emission Spectrometer

    Capable of handling even the most difficult, high-matrix samples without dilution, PerkinElmer’s Avio® 200 hybrid-scanning system brings a whole new level of performance and flexibility to ICP. What's more, that unprecedented performance comes with unparalleled ease-of-use. Unique hardware features and the industry’s most intuitive software combine to make multi-element measurements as easy as single-element analyses.

    The smallest ICP on the market, Avio 200 offers efficient operation, reliable data, and low cost of ownership by delivering:

  • The lowest argon consumption of any ICP
  • The fastest ICP startup (spectrometer ready in just minutes from power on)
  • Superior sensitivity and resolution for all elements of interest
  • Extended linear range with dual viewing technology
  • Download the brochure to learn more about the unique capabilities and benefits of PerkinElmer's Avio 200 hybrid-scanning ICP-OES.

  • Application Note

    Characterization of TiO2 Nanoparticle Release from Fabrics By Single Particle ICP-MS

    In the textile industry, the use of titanium dioxide (TiO2) nanoparticles (NPs) is increasing due to their ability to provide UV protection, increase the hydrophilic nature of fabrics, provide antibacterial characteristics, and reduce odors. This work demonstrates the ability of PerkinElmer's NexION® Single Particle ICP-MS with Syngistix Nano Application Software Module to both detect and measure TiO2 nanoparticles released from textiles.

  • Flyer

    NexSAR HPLC-ICP-MS Speciation Solution

    Speciation studies can provide comprehensive information regarding ion mobility, bioavailability, and toxicity. Consequently, many modern labs are expanding their analytical portfolio to include HPLC-ICP-MS. For such studies, it is advantageous to have an intuitive, user-friendly system that meets the user requirements for automation, ultra-low baseline, powerful integration, and flexible data export. And no one offers a more integrated, versatile, and inert speciation solution than PerkinElmer - accelerate your speciation analysis with the NexSAR? HPLC-ICP-MS Speciation Solution.

  • Application Note

    Analysis of SiO2- and TiO2-Containing Medications Using ICP-OES Following USP 232/233 Guidelines with Software Designed to Aid in 21 CFR Part 11 Compliance

    This work demonstrates the ability of the Avio 200 ICP-OES to meet the USP <232>/<233> criteria for Class 1 and 2A elements in tablets containing TiO2 or SiO2 as excipients using Syngistix for ICP Enhanced Security software version 4.0 for 21 CFR Part 11 compliance.

  • Application Note

    Advantages of a High Throughput Sample Introduction System in the Analysis of Drinking Waters Using ICP-MS (Method 200.8)

    This Application note reports the analysis of a number of water samples comprised of tap and natural waters in accordancewith the EPA Method 200.8 using PerkinElmer’s High Throughput System (HTS), which is fully-integrated with the NexION® ICP-MS using Syngistix for ICP-MS software.

  • White Paper

    Weighing the Benefits and Risks of Nanotechnology White Paper

    There is a growing body of evidence showing that there are significant differences between some nanomaterials and their non-nanoscale counterparts. What those differences portend raises many new questions about their potential to cause harm to human health and the environment.

  • Application Note

    Digestion, Testing, and Validation of Heavy Metals in Cannabis

    Owing to the toxicity of heavy metals, it is increasingly important to test cannabis flowers and other cannabis derivatives so that patient and consumer safety is maintained as the use of cannabis becomes more common. This need has translated into an increasing demand for testing cannabis flowers and other cannabis derivatives for toxins such as the heavy metals cadmium (Cd), lead (Pb), arsenic (As), and mercury (Hg). In this application note, we present data to illustrate the successful validation of the Titan MPS Microwave Sample Preparation System and the NexION® ICP-MS for the determination of heavy metals in cannabis flower according to the validation protocols set in USP General Chapter <233>, which are commonly used for evaluation of the levels of elemental impurities in samples.

  • Application Note

    Quantification of Nanoparticle Uptake into Cancer Cells using Single Cell ICP-MS

    Nanoparticles (NPs) have been of significant interest over the last two decades as they offer attractive benefits for drug delivery to overcome limitations in conventional chemotherapy. Nanoparticles can be engineered to carry both drugs and imaging probes to simultaneously detect and treat cancer. They may also be designed to specifically target diseased tissues and cells in the body. A number of nanoparticlebased cancer therapeutics have been approved for clinical use and/or are currently under development.

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